Titel: Multifunctional carbon-nanotube supported catalyst for efficient glycerol hydrogenolysis to 1,2-propanediol - Research data DOI of the publication: doi.org/10.1002/cctc.202501748 DOI: doi.org/10.15480/882.16291 Created by Dominique Lumpp Contributing researchers: - Dominique Lumpp, 0009-0008-4083-0355, dominique.lumpp@uni-hamburg.de, Institute of Technical and Macromolecular Chemistry, University of Hamburg, Hamburg, Germany - Samrin Shaikh, 0000-0001-8929-572X, samrin.shaikh@uni-hamburg.de, Institute of Technical and Macromolecular Chemistry, University of Hamburg, Hamburg, Germany - Fabian Riebesehl, 0009-0003-2611-7688, fabian.riebesehl@tuhh.de, Institute of Polymers and Composites, Hamburg University of Technology, Denickestraße 15, 21073 Hamburg, Germany - Charlotte Ruhmlieb, 0000-0002-1685-9827, charlotte.ruhmlieb@uni-hamburg.de, Institute of Physical Chemistry, University of Hamburg, Grindelallee 117, 20146 Hamburg, Germany - Kai Kruber, 0000-0002-6557-5396, kai.kruber@tuhh.de, Institute of Process Systems Engineering, Hamburg University of Technology, Am Schwarzenberg-Campus 4, 21073 Hamburg - Baldur Schroeter, 0000-0002-2577-055X, baldur.schroeter@tuhh.de, Institute of Thermal Separation Processes, Hamburg University of Technology, Eißendorfer Straße 38, 21073 Hamburg - Irina Smirnova, 0000-0003-4503-4039, irina.smirnova@tuhh.de, Institute of Thermal Separation Processes, Hamburg University of Technology, Eißendorfer Straße 38, 21073 Hamburg - Mirko Skiborowski, 0000-0001-9694-963X, mirko.skiborowski@tuhh.de, Institute of Process Systems Engineering, Hamburg University of Technology, Am Schwarzenberg-Campus 4, 21073 Hamburg - Bodo Fiedler, 0000-0002-2734-1353, fiedler@tuhh.de, Institute of Polymers and Composites, Hamburg University of Technology, Denickestraße 15, 21073 Hamburg, Germany - Jakob Albert, 0000-0002-3923-2269, jakob.albert@uni-hamburg.de, Institute of Technical and Macromolecular Chemistry, University of Hamburg, Hamburg, Germany Version 1.0 created 10.03.2026 Relevant research data: - TGA data of CNTs and Catalysts - Physisorption of CNTs and Catalysts - SEM and TEM pictures of CNTs and Catalysts - EDX mapping of CNTs and Catalysts - Chemisorption and TPR of Catalysts - p-XRD of Catalysts - Oven method and report files - HPLC batch, method and data files - GC method and report files - Files from SEM, TEM, XPS, - Raman measurements of CNT and Catalyst - FTIR measurements of CNTs and Catalyst - ICP-OES/ ICP-MS of CNTs and Catalysts - Lists of Catalysts and Experiments - NMR-spectra from reaction solution Used Software for data processing: Mestrenova 14.1.0-24037 for NMR data X’Pert HighScore Plus 2.2e XRD data Origin 2022 for data plotting Excel 2019 for calculations Shimadzu Lab Solutions Version 5.124 to use the HPLC Shimadzu Lab Solutions IR Version 2.26 to use the FT-IR Galaxie Sequence Manager 1.9.302.530 to use the GC TPRWin for Pulsar and ChemBet TPD-TPR 4.1 to use the chemisorption NovaWin 11.06 to look at physisorption data ImageJ 1.54g to further analyze SEM/TEM pictures Data fromates used: - PDF File from EDX and ICP results - CFG File - QTP File from TPR measurements - DATA File - Shimadzu LabSolutions LC/LCMS Method File from HPLC - Shimadzu LabSolutions LC/LCMS Data File from HPLC - Shimadzu LabSolutions LC/LCMS Batch File from HPLC - Text Document from TPR and Physisorption measurements - Origin File for data plotting - Excel Files from ICP of UHH - Word File for workplans, result summary - MNova File for NMR spectra - XRDML File for XRD spectra - jpg pictures by SEM and TEM - tif pictures by SEM and TEM - pptx for Presentations internally and externally Data sources: GC Data is generated by a Varian 450-GC as text file or PDF report HPLC Data is generated by HPLC-LC System TPR and Chemisorption data is generated by ChemBET Pulsar TPR/TPD IR data is generated by IRSpirit by Shimadzu ICP-OES Data is generated by inductively coupled plasma optical emission spectrometer (ICP-OES, Perkin Elmer, Avio 550) XPS Data is generated by ESCALAB 220iXL (ThermoFischer Scientific) PXRD is generated by Panalytical MDP X'Pert Pro diffractometer SEM and EDX data are generated by LEO Gemini 1550 (Zeiss) HRTEM data is generated by JEM-2200FS (JEOL) TEM N2-physisorption data is generated by Nova 3000e Surface Area Analyzer, Quantachrome Instruments This data set contain the research data for the publication Multifunctional carbon-nanotube supported catalyst for efficient glycerol hydrogenolysis to 1,2-propanediol In this publication a carbon nanotube supported catalyst for the hydrogenolysis of glycerol was developed. The data set is divided into two different sets. The first set, activity studies contains all data for the evaluation of the catalytic activity, like HPLC, GC, NMR data and the calculations for the Experiment. There is a list that gives an overview over all experiments and a seperate folder for each experiment. Metadata regarding the experiments can be found in the excel files. The second folder contains all data relevant for the catalyst analytics. There is a list where all catalysts are mentioned and a folder for each catalyst analysis data, were the raw data is stored.