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  4. XRD and GC data for oxidative dehydrogenation of ethane (IPO-XRD study)
 
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XRD and GC data for oxidative dehydrogenation of ethane (IPO-XRD study)

Citation Link: https://doi.org/10.15480/882.16940
Type
Dataset
Version
1
Date Issued
2026-04-17
Author(s)
Gizer, Gökhan 
Chemische Reaktionstechnik V-2  
Zeeshan, Hafiz Muhammad  
Chemische Reaktionstechnik V-2  
Contact
Horn, Raimund  
Chemische Reaktionstechnik V-2  
Language
English
DOI
https://doi.org/10.15480/882.16940
TORE-URI
https://hdl.handle.net/11420/62500
Abstract
The approach is demonstrated for the oxidative dehydrogenation of ethane over a 30 wt% MoO3/γ − Al2O3 catalyst, a system exhibiting pronounced and reversible structural dynamics. IPO-XRD captures the spatial transition from oxidized molybdenum phases (Al2(MoO4)3 and Mo-suboxides) to reduced MoO2, directly linked to the depletion of gas-phase oxygen. Excellent agreement between iso-potential measurements and direct reactor measurements at a synchrotron confirms the validity of the concept, while additional experiments on a laboratory diffractometer demonstrate its broader applicability.
Subjects
Iso potential operando spectoscopy
Heterogeneous Catalysis
X-ray diffraction
Profile reactor
Catalyst structural dynamics
DDC Class
541.3: Physical Chemistry
Funding(s)
SFB 1615 - Teilprojekt B02: In situ Diagnose und Kontrolle der Elektrobenetzung von Kohlenstoffnanoröhrchen-Katalysatoren für die Anwendung in Mehrphasenreaktoren  
Funding Organisations
Deutsche Forschungsgemeinschaft (DFG)  
More Funding Information
This project is funded by the Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) – SFB 1615 – 503850735.
License
https://creativecommons.org/publicdomain/zero/1.0/
Technical information
License for Use:
- Raw data files (.asc, .opju, .xlsx, .csv): Public Domain Mark (PDM)
- Figures (.png): CC BY 4.0
No Thumbnail Available
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XRD_data.zip

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5.05 MB

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ZIP

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GC_data.zip

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381.59 KB

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ZIP

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Figures.zip

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20.28 MB

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ZIP

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XRD_GC_ODH_ethane_IPO_XRD.zip

Size

25.72 MB

Format

ZIP

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