Hofmann, TommyTommyHofmannWallacher, DirkDirkWallacherHuber, PatrickPatrickHuberBirringer, RainerRainerBirringerKnorr, KlausKlausKnorrSchreiber, AndreasAndreasSchreiberFindenegg, Gerhard H.Gerhard H.Findenegg2022-06-032022-06-032005-08-01Physical Review B - Condensed Matter and Materials Physics 72 (6): 064122 (2005-08-01)http://hdl.handle.net/11420/12807Kr has been adsorbed in SBA-15, a template-grown mesoporous silica substrate. A volumetric adsorption isotherm is presented. The Bragg peaks of the pore array have been measured by small angle x-ray diffraction and analyzed as function of the filling fraction in terms of the electron density contrast, the radial position of the liquid-vapor interface, and film roughness, both for the regime of film growth and capillary condensation. The results are compared with the theory of Saam and Cole. It is shown that the microporosity of the matrix leads to a delay of capillary condensation. The peculiar dependence of the film thickness on the filling fraction points to a high fractal dimension of the pore walls. © 2005 The American Physical Society.en1550-235X20056American Physical SocietyPhysikChemieJournal Article10.1103/PhysRevB.72.064122Journal Article