May, ManfredManfredMayBoderius, MathisMathisBoderiusGostkowska-Lekner, NataliaNataliaGostkowska-LeknerBusch, MarkMarkBuschHabicht, KlausKlausHabichtHofmann, TommyTommyHofmannHuber, PatrickPatrickHuber2024-01-162024-01-162024-01-16https://hdl.handle.net/11420/45099Dataset that contains different data on electrochemical and x-ray diffraction experiments of the synthesis and structure investigations of hybrid materials made out of conductive polymers and porous silicon. The mesoporous silicon epilayers are filled electrochemically with the polymers polypyrrole and poly-3,4-ethylendioxythiophen. Polyaniline could only be deposited on top of the porous silicon and not inside the mesopores. If applicable, the galvanostatic raw datasets have to normalized by the epilayer surface area of 7.89cm². The x-ray diffraction data contains both powder diffraction data sets (counts vs. 2-theta) and 2D detector images (P08 DESY synchrotron, 25 keV) of the monomer 2,5-Dibromo-3,4-ethylenedioxythiophene and the polymer poly-3,4-ethylendioxythiophen after solid state polymerization at 60°C. The samples investigated at the synchrotron (2D datasets) are hybrid materials in which the mesoporous pore space of the silicon is filled via spontaneous imbibition of the DBEDOT and subsequently polymerized to PEDOT. Each 2D image is taken at a different z position in order to mitigate beam damage.enhttps://creativecommons.org/publicdomain/mark/1.0/X-ray diffractionelectrochemical synthesis of organic-inorganic hybridsconductive polymerssolid state polyermizationmesoporous siliconEngineering and Applied OperationsChemistryExperimental Data10.15480/882.904910.15480/882.9049May, ManfredManfredMayMay, ManfredManfredMay10.1016/j.micromeso.2024.11318110.15480/882.13065Deutsches Elektronen-Synchrotron DESY