TUHH Open Research
Help
  • Log In
    New user? Click here to register.Have you forgotten your password?
  • English
  • Deutsch
  • Communities & Collections
  • Publications
  • Research Data
  • People
  • Institutions
  • Projects
  • Statistics
  1. Home
  2. TUHH
  3. Research Data
  4. Wafer-scale fabrication of mesoporous silicon functionalized with electrically conductive polymers
 
Options

Wafer-scale fabrication of mesoporous silicon functionalized with electrically conductive polymers

Citation Link: https://doi.org/10.15480/882.9049
Type
Experimental Data
Date Issued
2024-01-16
Author(s)
May, Manfred  
Material- und Röntgenphysik M-2  
Boderius, Mathis  
Studiendekanat Maschinenbau  
Gostkowska-Lekner, Natalia  
Helmholtz-Zentrum Berlin für Materialien und Energie  
Busch, Mark  orcid-logo
Material- und Röntgenphysik M-2  
Habicht, Klaus  
Helmholtz-Zentrum Berlin für Materialien und Energie  
Hofmann, Tommy  orcid-logo
Helmholtz-Zentrum Berlin für Materialien und Energie  
Huber, Patrick  orcid-logo
Material- und Röntgenphysik M-2  
Researcher
Bertram, Florian  
Data Collector
May, Manfred  
Contact
May, Manfred  
Data Collector
Deutsches Elektronen-Synchrotron DESY  
Language
English
DOI
10.15480/882.9049
TORE-URI
https://hdl.handle.net/11420/45099
Is Supplement To
10.1016/j.micromeso.2024.113181
10.15480/882.13065
Abstract
Dataset that contains different data on electrochemical and x-ray diffraction experiments of the synthesis and structure investigations of hybrid materials made out of conductive polymers and porous silicon. The mesoporous silicon epilayers are filled electrochemically with the polymers polypyrrole and poly-3,4-ethylendioxythiophen. Polyaniline could only be deposited on top of the porous silicon and not inside the mesopores. If applicable, the galvanostatic raw datasets have to normalized by the epilayer surface area of 7.89cm². The x-ray diffraction data contains both powder diffraction data sets (counts vs. 2-theta) and 2D detector images (P08 DESY synchrotron, 25 keV) of the monomer 2,5-Dibromo-3,4-ethylenedioxythiophene and the polymer poly-3,4-ethylendioxythiophen after solid state polymerization at 60°C. The samples investigated at the synchrotron (2D datasets) are hybrid materials in which the mesoporous pore space of the silicon is filled via spontaneous imbibition of the DBEDOT and subsequently polymerized to PEDOT. Each 2D image is taken at a different z position in order to mitigate beam damage.
Subjects
X-ray diffraction
electrochemical synthesis of organic-inorganic hybrids
conductive polymers
solid state polyermization
mesoporous silicon
DDC Class
620: Engineering
540: Chemistry
Funding(s)
Hybrid Thermoelectric Materials Based on Porous Silicon: Linking Macroscopic Transport Phenomena to Microscopic Structure and Elementary Excitations  
SFB 986: Tailor-Made Multi-Scale Materials Systems - M3  
DESY Beamtime I-20210755
License
https://creativecommons.org/publicdomain/mark/1.0/
No Thumbnail Available
Name

Fig1b1_galvanostatic_1,9992mA_PPyprimer.txt

Size

98.06 KB

Format

Text

No Thumbnail Available
Name

Fig1b2_galvanostatic_1,9992mA_PPyfull.txt

Size

769.61 KB

Format

Text

No Thumbnail Available
Name

Fig6a_PEDOT_powder_EtOH.txt

Size

55.63 KB

Format

Text

No Thumbnail Available
Name

Fig6a_DBEDOT_powder.txt

Size

55.63 KB

Format

Text

No Thumbnail Available
Name

Fig6a_PEDOT_powder_24h60C.txt

Size

55.63 KB

Format

Text

No Thumbnail Available
Name

Fig1c_galvanostatic_2mA_PEDOTwithoutPPyprimer.txt

Size

2.02 MB

Format

Text

No Thumbnail Available
Name

Fig3_CV_-0,6Vbis0,95V_20mVHz_PANI_3M_Ethanol.txt

Size

472.57 KB

Format

Text

No Thumbnail Available
Name

Fig4_blue_potentiostatic_0,9V_PANI.txt

Size

427.44 KB

Format

Text

No Thumbnail Available
Name

Fig4black_galvanostatic_2mA_PANI.txt

Size

6.08 MB

Format

Text

No Thumbnail Available
Name

Fig6_calibration_lab6.tif

Size

16 MB

Format

TIFF

TUHH
Weiterführende Links
  • Contact
  • Send Feedback
  • Cookie settings
  • Privacy policy
  • Impress
DSpace Software

Built with DSpace-CRIS software - Extension maintained and optimized by 4Science
Design by effective webwork GmbH

  • Deutsche NationalbibliothekDeutsche Nationalbibliothek
  • ORCiD Member OrganizationORCiD Member Organization
  • DataCiteDataCite
  • Re3DataRe3Data
  • OpenDOAROpenDOAR
  • OpenAireOpenAire
  • BASE Bielefeld Academic Search EngineBASE Bielefeld Academic Search Engine
Feedback